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Effect of blend composition on the morphology development of electrospun fibres based on PAN/PMMA blends

  • Chang Kook Hong
  • , Kap Seung Yang
  • , Seung Hyun Oh
  • , Jou Hyeon Ahn
  • , Baik Hwan Cho
  • , Changwoon Nah*
  • *Corresponding author for this work
  • Chonnam National University
  • Jeonbuk National University
  • Gyeongsang National University

Research output: Contribution to journalJournal articlepeer-review

Abstract

Background: The aim of the work presented was to determine the morphology development and relevant change in fibre diameter of a binary polymer blend system during an electrospinning process. The size of the fibre diameter is one of the important factors determining the general properties of non-woven mats formed from electrospun fibres. Results: The morphology and diameter of electrospun polyacrylonitrile (PAN)/poly(methyl methacrylate) (PMMA) blends were investigated as a function of blend ratio using scanning electron microscopy. The diameter of the electrospun PAN/PMMA fibres decreased with increasing PMMA content up to 50 wt%, and then increased again with further increase of PMMA. After thermal treatment, the fibres shrank, and an irregularly shaped morphology was observed. Conclusion: The electrospinning of incompatible PAN/PMMA blends leads to a microphase-separation morphology of fibres. A phase inversion occurs at a PMMA content of between 50 and 75 wt%. Due to the phase inversion, the fibre diameter shows a minimum value at the relevant composition.

Original languageEnglish
Pages (from-to)1357-1362
Number of pages6
JournalPolymer International
Volume57
Issue number12
DOIs
StatePublished - 2008

Keywords

  • Diameter
  • Electrospinning
  • Morphology
  • PAN/PMMA blend
  • Viscosity

Quacquarelli Symonds(QS) Subject Topics

  • Materials Science
  • Engineering - Petroleum
  • Chemistry

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