Low temperature synthesis and characterization of rosette-like nanostructures of ZnO using solution process

Rizwan Wahab; S. G. Ansari; Hyung Kee Seo; Young Soon Kim; Eun Kyung Suh; Hyung Shik Shin

doi:10.1016/j.solidstatesciences.2008.07.009

Low temperature synthesis and characterization of rosette-like nanostructures of ZnO using solution process

Rizwan Wahab
, S. G. Ansari
, Hyung Kee Seo
, Young Soon Kim
, Eun Kyung Suh
, Hyung Shik Shin^*

^*Corresponding author for this work

Division of Chemical Engineering

Jeonbuk National University

Research output: Contribution to journal › Journal article › peer-review

59 Scopus citations

Abstract

Rosette-like structures of ZnO were synthesized at low temperature (60 °C) using solution process over 20 min of time. Hydroxylamine hydrochloride was used as capping agent with zinc nitrate hexahydrate and sodium hydroxide. Transition from triangular shaped plate like particles to rosette-like structure and to individual nanorods is observed with increasing refluxing temperature. Single-crystalline nature with wurtzite hexagonal phase is confirmed from transmission electron microscopic observations. Photoelectron spectroscopic measurement presented spectra close to the standard bulk ZnO, with an O 1s peak composed of surface adsorbed O-H group, O^2- in the oxygen vacancies on ZnO structure and ZnO.

Original language	English
Pages (from-to)	439-443
Number of pages	5
Journal	Solid State Sciences
Volume	11
Issue number	2
DOIs	https://doi.org/10.1016/j.solidstatesciences.2008.07.009
State	Published - 2009.02

Keywords

Low temperature
Rosette-like structures
Solution process
ZnO

Quacquarelli Symonds(QS) Subject Topics

Materials Science
Chemistry
Physics & Astronomy

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10.1016/j.solidstatesciences.2008.07.009

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@article{2187871649084922952ba048c9f83cd8,

title = "Low temperature synthesis and characterization of rosette-like nanostructures of ZnO using solution process",

abstract = "Rosette-like structures of ZnO were synthesized at low temperature (60 °C) using solution process over 20 min of time. Hydroxylamine hydrochloride was used as capping agent with zinc nitrate hexahydrate and sodium hydroxide. Transition from triangular shaped plate like particles to rosette-like structure and to individual nanorods is observed with increasing refluxing temperature. Single-crystalline nature with wurtzite hexagonal phase is confirmed from transmission electron microscopic observations. Photoelectron spectroscopic measurement presented spectra close to the standard bulk ZnO, with an O 1s peak composed of surface adsorbed O-H group, O2- in the oxygen vacancies on ZnO structure and ZnO.",

keywords = "Low temperature, Rosette-like structures, Solution process, ZnO",

author = "Rizwan Wahab and Ansari, \{S. G.\} and Seo, \{Hyung Kee\} and Kim, \{Young Soon\} and Suh, \{Eun Kyung\} and Shin, \{Hyung Shik\}",

year = "2009",

month = feb,

doi = "10.1016/j.solidstatesciences.2008.07.009",

language = "English",

volume = "11",

pages = "439--443",

journal = "Solid State Sciences",

issn = "1293-2558",

number = "2",

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TY - JOUR

T1 - Low temperature synthesis and characterization of rosette-like nanostructures of ZnO using solution process

AU - Wahab, Rizwan

AU - Ansari, S. G.

AU - Seo, Hyung Kee

AU - Kim, Young Soon

AU - Suh, Eun Kyung

AU - Shin, Hyung Shik

PY - 2009/2

Y1 - 2009/2

N2 - Rosette-like structures of ZnO were synthesized at low temperature (60 °C) using solution process over 20 min of time. Hydroxylamine hydrochloride was used as capping agent with zinc nitrate hexahydrate and sodium hydroxide. Transition from triangular shaped plate like particles to rosette-like structure and to individual nanorods is observed with increasing refluxing temperature. Single-crystalline nature with wurtzite hexagonal phase is confirmed from transmission electron microscopic observations. Photoelectron spectroscopic measurement presented spectra close to the standard bulk ZnO, with an O 1s peak composed of surface adsorbed O-H group, O2- in the oxygen vacancies on ZnO structure and ZnO.

AB - Rosette-like structures of ZnO were synthesized at low temperature (60 °C) using solution process over 20 min of time. Hydroxylamine hydrochloride was used as capping agent with zinc nitrate hexahydrate and sodium hydroxide. Transition from triangular shaped plate like particles to rosette-like structure and to individual nanorods is observed with increasing refluxing temperature. Single-crystalline nature with wurtzite hexagonal phase is confirmed from transmission electron microscopic observations. Photoelectron spectroscopic measurement presented spectra close to the standard bulk ZnO, with an O 1s peak composed of surface adsorbed O-H group, O2- in the oxygen vacancies on ZnO structure and ZnO.

KW - Low temperature

KW - Rosette-like structures

KW - Solution process

KW - ZnO

UR - https://www.scopus.com/pages/publications/58949088487

U2 - 10.1016/j.solidstatesciences.2008.07.009

DO - 10.1016/j.solidstatesciences.2008.07.009

M3 - Journal article

AN - SCOPUS:58949088487

SN - 1293-2558

VL - 11

SP - 439

EP - 443

JO - Solid State Sciences

JF - Solid State Sciences

IS - 2

ER -

Low temperature synthesis and characterization of rosette-like nanostructures of ZnO using solution process

Abstract

Keywords

Quacquarelli Symonds(QS) Subject Topics

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