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Preparation of coil-embolic material using syndiotactic poly(vinyl alcohol) gel spun fibers

  • Young Ho Seo
  • , Tae Hwan Oh*
  • , Sung Soo Han
  • , Sang Woo Joo
  • , Myeong Seob Khil
  • *Corresponding author for this work
  • Yeungnam University

Research output: Contribution to journalJournal articlepeer-review

Abstract

The structure, morphology, and physical properties of syndiotatic poly(vinyl alcohol) (s-PVA) gel spun fibers were investigated to prepare polymeric embolization coils. S-PVA was prepared by saponification of the poly(vinyl acetate)/poly(vinyl pivalate)(PVAc/PVPi) copolymer. The viscosity of s-PVA solutions showed shear thinning behavior and the solution formed a homogeneous phase. Based on shear viscosity change with concentration, the optimum dope concentration was selected as 13 wt%, after which s-PVA fibers were spun and the solvent was removed. The fibers were then drawn with a maximum draw ratio of 15. A polymeric embolization coil was made of the s-PVA gel-spun fibers. The fibers were wound densely onto rigid rod and then annealed at different annealing temperatures. The polymeric embolization coil annealed at 200 °C was similar to metallic coils and its shape was maintained well after extension. Overall, gel-spun PVA fibers performed well for the preparation of primary and secondary coils to replace metallic coils.

Original languageEnglish
Pages (from-to)486-493
Number of pages8
JournalPolymer (Korea)
Volume37
Issue number4
DOIs
StatePublished - 2013.07

Keywords

  • Coil
  • Draw ratio
  • Embolization
  • Gel spun fibers
  • S-PVA

Quacquarelli Symonds(QS) Subject Topics

  • Materials Science
  • Engineering - Chemical

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