Processing of soju industrial bioresidue to extract microcrystalline cellulose and characterization

A. Naidu Bhima; J. H. Park; M. Cho; S. G. Oh; H. Myung; S. Kamala-Kannan; B. T. Oh

doi:10.3139/217.2996

Processing of soju industrial bioresidue to extract microcrystalline cellulose and characterization

A. Naidu Bhima
, J. H. Park
, M. Cho
, S. G. Oh
, H. Myung
, S. Kamala-Kannan
, B. T. Oh^*

^*Corresponding author for this work

Research output: Contribution to journal › Journal article › peer-review

Abstract

Soju industrial biomass residue (SIBR) is a lignocellulosic agro-industrial biowaste available in large quantities in soju producing countries. In this study, an attempt was made to extract microcrystalline cellulose (MCC), a biopolymer from SIBR by controlled acid hydrolysis. X-ray diffraction analysis indicated the presence of cellulose I structure with two peaks around 2θ = 15 and 22.5° and increase in crystallinity after acid hydrolysis treatment. Fourier transform infrared analysis showed no significant chemical affect of the cellulose fragment. Thermo-gravimetric analysis reveals that the extracted MCC have a good thermal stability (319°C). Dynamic light scattering studies confirmed the presence of MCC in micro range (126.4 nm) which was supported by transmission electron microscopy. The results of this work are useful for extracting valuable and widely applicable cellulose, and help solve management of SIBR in terms of disposal and pollution problems.

Original language	English
Pages (from-to)	337-343
Number of pages	7
Journal	International Polymer Processing
Volume	30
Issue number	3
DOIs	https://doi.org/10.3139/217.2996
State	Published - 2015.07

Quacquarelli Symonds(QS) Subject Topics

Materials Science
Engineering - Mechanical
Engineering - Chemical

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@article{cd345e64545642e8a78dcf3eeda3ceb0,

title = "Processing of soju industrial bioresidue to extract microcrystalline cellulose and characterization",

abstract = "Soju industrial biomass residue (SIBR) is a lignocellulosic agro-industrial biowaste available in large quantities in soju producing countries. In this study, an attempt was made to extract microcrystalline cellulose (MCC), a biopolymer from SIBR by controlled acid hydrolysis. X-ray diffraction analysis indicated the presence of cellulose I structure with two peaks around 2θ = 15 and 22.5° and increase in crystallinity after acid hydrolysis treatment. Fourier transform infrared analysis showed no significant chemical affect of the cellulose fragment. Thermo-gravimetric analysis reveals that the extracted MCC have a good thermal stability (319°C). Dynamic light scattering studies confirmed the presence of MCC in micro range (126.4 nm) which was supported by transmission electron microscopy. The results of this work are useful for extracting valuable and widely applicable cellulose, and help solve management of SIBR in terms of disposal and pollution problems.",

author = "\{Naidu Bhima\}, A. and Park, \{J. H.\} and M. Cho and Oh, \{S. G.\} and H. Myung and S. Kamala-Kannan and Oh, \{B. T.\}",

note = "Publisher Copyright: {\textcopyright} 2015 Carl Hanser Verlag GmbH \& Co. KG.",

year = "2015",

month = jul,

doi = "10.3139/217.2996",

language = "English",

volume = "30",

pages = "337--343",

journal = "International Polymer Processing",

issn = "0930-777X",

number = "3",

}

TY - JOUR

T1 - Processing of soju industrial bioresidue to extract microcrystalline cellulose and characterization

AU - Naidu Bhima, A.

AU - Park, J. H.

AU - Cho, M.

AU - Oh, S. G.

AU - Myung, H.

AU - Kamala-Kannan, S.

AU - Oh, B. T.

PY - 2015/7

Y1 - 2015/7

N2 - Soju industrial biomass residue (SIBR) is a lignocellulosic agro-industrial biowaste available in large quantities in soju producing countries. In this study, an attempt was made to extract microcrystalline cellulose (MCC), a biopolymer from SIBR by controlled acid hydrolysis. X-ray diffraction analysis indicated the presence of cellulose I structure with two peaks around 2θ = 15 and 22.5° and increase in crystallinity after acid hydrolysis treatment. Fourier transform infrared analysis showed no significant chemical affect of the cellulose fragment. Thermo-gravimetric analysis reveals that the extracted MCC have a good thermal stability (319°C). Dynamic light scattering studies confirmed the presence of MCC in micro range (126.4 nm) which was supported by transmission electron microscopy. The results of this work are useful for extracting valuable and widely applicable cellulose, and help solve management of SIBR in terms of disposal and pollution problems.

AB - Soju industrial biomass residue (SIBR) is a lignocellulosic agro-industrial biowaste available in large quantities in soju producing countries. In this study, an attempt was made to extract microcrystalline cellulose (MCC), a biopolymer from SIBR by controlled acid hydrolysis. X-ray diffraction analysis indicated the presence of cellulose I structure with two peaks around 2θ = 15 and 22.5° and increase in crystallinity after acid hydrolysis treatment. Fourier transform infrared analysis showed no significant chemical affect of the cellulose fragment. Thermo-gravimetric analysis reveals that the extracted MCC have a good thermal stability (319°C). Dynamic light scattering studies confirmed the presence of MCC in micro range (126.4 nm) which was supported by transmission electron microscopy. The results of this work are useful for extracting valuable and widely applicable cellulose, and help solve management of SIBR in terms of disposal and pollution problems.

UR - https://www.scopus.com/pages/publications/84957067959

U2 - 10.3139/217.2996

DO - 10.3139/217.2996

M3 - Journal article

AN - SCOPUS:84957067959

SN - 0930-777X

VL - 30

SP - 337

EP - 343

JO - International Polymer Processing

JF - International Polymer Processing

IS - 3

ER -

Processing of soju industrial bioresidue to extract microcrystalline cellulose and characterization

Abstract

Quacquarelli Symonds(QS) Subject Topics

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