Structural and mechanical properties of cellulose acetate/graphene hybrid nanofibers: Spectroscopic investigations

  • M. Gopiraman
  • , K. Fujimori
  • , K. Zeeshan
  • , B. S. Kim
  • , I. S. Kim

Research output: Contribution to journalJournal articlepeer-review

Abstract

Cellulose acetate/graphene (CA/graphene) and cellulose acetate/graphene-COOH (CA/graphene-COOH) hybrid nanofibers were fabricated via electrospinning technique, and their morphologies, crystallinity and mechanical properties were investigated. The added amounts of graphene and graphene-COOH were varied from 0.5 to 5.0 wt%. The crystal structures and morphologies of the resultant hybrid nanofibers were investigated by wide angle X-ray diffraction (WAXD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM), respectively. Graphene-COOH incorporated CA nanofiber mats showed higher Young's modulus of about 910 MPa among than those of CA/graphene nanofibers, which is due to molecular interactions between -COOH groups in acid-treated graphene and C=O groups in CA via hydrogen bonding. This specific interaction was demonstrated by spectroscopic studies (Raman and Fourier transform infrared (FT-IR) spectroscopies).

Original languageEnglish
Pages (from-to)554-563
Number of pages10
JournalExpress Polymer Letters
Volume7
Issue number6
DOIs
StatePublished - 2013.06

Keywords

  • Graphene
  • Mechanical properties
  • Molecular interactions
  • Nanofiber
  • Polymer composites

Quacquarelli Symonds(QS) Subject Topics

  • Materials Science
  • Engineering - Petroleum
  • Engineering - Chemical
  • Chemistry

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