The preparation of butyrylated NAD+ type of biological molecules

Ki Jun Hwang; Beom Tae Kim; Uh Hyun Kim

doi:10.1081/SCC-120022168

The preparation of butyrylated NAD⁺ type of biological molecules

Ki Jun Hwang^*
, Beom Tae Kim
, Uh Hyun Kim

^*Corresponding author for this work

Department of Bioenvironmental Chemistry

Jeonbuk National University
College of Natural Science

Research output: Contribution to journal › Journal article › peer-review

Abstract

Butyrylated NAD⁺ and its fluorescent analog, 1,N⁶-etheno NAD⁺ are prepared in good yields by employing two-phase system, i.e., water and CH₂Cl₂ containing dimethyaminopyridine and excess butyric anhydride. The reaction condition for this reaction is so specific that several other acylating conditions attempted were totally failed, and this developed methodology will be conveniently utilized for the further study of cyclic ADP-ribose (cADPR).

Original language	English
Pages (from-to)	2803-2810
Number of pages	8
Journal	Synthetic Communications
Volume	33
Issue number	16
DOIs	https://doi.org/10.1081/SCC-120022168
State	Published - 2003

Quacquarelli Symonds(QS) Subject Topics

Engineering - Petroleum
Chemistry

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10.1081/SCC-120022168

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title = "The preparation of butyrylated NAD+ type of biological molecules",

abstract = "Butyrylated NAD+ and its fluorescent analog, 1,N6-etheno NAD+ are prepared in good yields by employing two-phase system, i.e., water and CH2Cl2 containing dimethyaminopyridine and excess butyric anhydride. The reaction condition for this reaction is so specific that several other acylating conditions attempted were totally failed, and this developed methodology will be conveniently utilized for the further study of cyclic ADP-ribose (cADPR).",

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year = "2003",

doi = "10.1081/SCC-120022168",

language = "English",

volume = "33",

pages = "2803--2810",

journal = "Synthetic Communications",

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number = "16",

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T1 - The preparation of butyrylated NAD+ type of biological molecules

AU - Hwang, Ki Jun

AU - Kim, Beom Tae

AU - Kim, Uh Hyun

PY - 2003

Y1 - 2003

N2 - Butyrylated NAD+ and its fluorescent analog, 1,N6-etheno NAD+ are prepared in good yields by employing two-phase system, i.e., water and CH2Cl2 containing dimethyaminopyridine and excess butyric anhydride. The reaction condition for this reaction is so specific that several other acylating conditions attempted were totally failed, and this developed methodology will be conveniently utilized for the further study of cyclic ADP-ribose (cADPR).

AB - Butyrylated NAD+ and its fluorescent analog, 1,N6-etheno NAD+ are prepared in good yields by employing two-phase system, i.e., water and CH2Cl2 containing dimethyaminopyridine and excess butyric anhydride. The reaction condition for this reaction is so specific that several other acylating conditions attempted were totally failed, and this developed methodology will be conveniently utilized for the further study of cyclic ADP-ribose (cADPR).

UR - https://www.scopus.com/pages/publications/0043131899

U2 - 10.1081/SCC-120022168

DO - 10.1081/SCC-120022168

M3 - Journal article

AN - SCOPUS:0043131899

SN - 0039-7911

VL - 33

SP - 2803

EP - 2810

JO - Synthetic Communications

JF - Synthetic Communications

IS - 16

ER -

The preparation of butyrylated NAD⁺ type of biological molecules

Abstract

Quacquarelli Symonds(QS) Subject Topics

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