Validation of bulk analysis with simulated swipe samples containing ultra-trace amounts of uranium and plutonium using MC-ICP-MS

Sang Ho Lim; Sun Ho Han; Jong Ho Park; Ranhee Park; Min Young Lee; Jinkyu Park; Chi Gyu Lee; Kyuseok Song

doi:10.5478/MSL.2015.6.3.75

Validation of bulk analysis with simulated swipe samples containing ultra-trace amounts of uranium and plutonium using MC-ICP-MS

Sang Ho Lim^*
, Sun Ho Han
, Jong Ho Park
, Ranhee Park
, Min Young Lee
, Jinkyu Park
, Chi Gyu Lee
, Kyuseok Song

^*Corresponding author for this work

Chemistry Education

Korea Atomic Energy Research Institute
University of Science and Technology UST

Research output: Contribution to journal › Journal article › peer-review

5 Scopus citations

Abstract

Suitable analytical procedures for the bulk analysis of ultra-trace amounts of uranium and plutonium have been developed using multi-collector inductively coupled mass spectrometry (MC–ICP–MS). The quantification and determination of the isotopic ratios of uranium and plutonium in three simulated swipe samples, a swipe blank, and a process blank were performed to validate the analytical performance. The analytical results for the simulated swipe samples were in good agreement with the certified values, based on the measurement quality goals for the analysis of bulk environmental samples recommended by the International Atomic Energy Agency (IAEA).

Original language	English
Pages (from-to)	75-79
Number of pages	5
Journal	Mass Spectrometry Letters
Volume	6
Issue number	3
DOIs	https://doi.org/10.5478/MSL.2015.6.3.75
State	Published - 2015.09

Keywords

Bulk analysis
Chemical separation
Environmental samples
IDMS
MC-ICP-MS

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10.5478/MSL.2015.6.3.75

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title = "Validation of bulk analysis with simulated swipe samples containing ultra-trace amounts of uranium and plutonium using MC-ICP-MS",

abstract = "Suitable analytical procedures for the bulk analysis of ultra-trace amounts of uranium and plutonium have been developed using multi-collector inductively coupled mass spectrometry (MC–ICP–MS). The quantification and determination of the isotopic ratios of uranium and plutonium in three simulated swipe samples, a swipe blank, and a process blank were performed to validate the analytical performance. The analytical results for the simulated swipe samples were in good agreement with the certified values, based on the measurement quality goals for the analysis of bulk environmental samples recommended by the International Atomic Energy Agency (IAEA).",

keywords = "Bulk analysis, Chemical separation, Environmental samples, IDMS, MC-ICP-MS",

author = "Lim, \{Sang Ho\} and Han, \{Sun Ho\} and Park, \{Jong Ho\} and Ranhee Park and Lee, \{Min Young\} and Jinkyu Park and Lee, \{Chi Gyu\} and Kyuseok Song",

year = "2015",

month = sep,

doi = "10.5478/MSL.2015.6.3.75",

language = "English",

volume = "6",

pages = "75--79",

journal = "Mass Spectrometry Letters",

issn = "2233-4203",

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T1 - Validation of bulk analysis with simulated swipe samples containing ultra-trace amounts of uranium and plutonium using MC-ICP-MS

AU - Lim, Sang Ho

AU - Han, Sun Ho

AU - Park, Jong Ho

AU - Park, Ranhee

AU - Lee, Min Young

AU - Park, Jinkyu

AU - Lee, Chi Gyu

AU - Song, Kyuseok

PY - 2015/9

Y1 - 2015/9

N2 - Suitable analytical procedures for the bulk analysis of ultra-trace amounts of uranium and plutonium have been developed using multi-collector inductively coupled mass spectrometry (MC–ICP–MS). The quantification and determination of the isotopic ratios of uranium and plutonium in three simulated swipe samples, a swipe blank, and a process blank were performed to validate the analytical performance. The analytical results for the simulated swipe samples were in good agreement with the certified values, based on the measurement quality goals for the analysis of bulk environmental samples recommended by the International Atomic Energy Agency (IAEA).

AB - Suitable analytical procedures for the bulk analysis of ultra-trace amounts of uranium and plutonium have been developed using multi-collector inductively coupled mass spectrometry (MC–ICP–MS). The quantification and determination of the isotopic ratios of uranium and plutonium in three simulated swipe samples, a swipe blank, and a process blank were performed to validate the analytical performance. The analytical results for the simulated swipe samples were in good agreement with the certified values, based on the measurement quality goals for the analysis of bulk environmental samples recommended by the International Atomic Energy Agency (IAEA).

KW - Bulk analysis

KW - Chemical separation

KW - Environmental samples

KW - IDMS

KW - MC-ICP-MS

UR - https://www.scopus.com/pages/publications/84993976472

U2 - 10.5478/MSL.2015.6.3.75

DO - 10.5478/MSL.2015.6.3.75

M3 - Journal article

AN - SCOPUS:84993976472

SN - 2233-4203

VL - 6

SP - 75

EP - 79

JO - Mass Spectrometry Letters

JF - Mass Spectrometry Letters

IS - 3

ER -

Validation of bulk analysis with simulated swipe samples containing ultra-trace amounts of uranium and plutonium using MC-ICP-MS

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Keywords

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